《分析测试技术与仪器》 2023 年（共 4 期，按页码顺序）总目录

* 分析测试新成果

氯化钾及聚乙二醇对聚脯氨酸-精氨酸液-液相分离的协同影响 ························································································································ 项东鑫，郑 寓，周诗航，陆 奕，王艳伟 （ 1 ）

交流电弧原子发射光谱固体粉末样品制备方法的改进 ·················· 郭心玮，郝志红，姚建贞，白金峰 （ 7 ）

分散固相萃取-超高效液相色谱-串联质谱法测定海龙中11 种磺胺类抗菌药物残留 ································································ 王小乔，李 坚，许晓辉，李剑勇，吴福祥，张虹艳，潘秀丽，李 赟 （ 16 ）

滤过型萃取柱-超高效液相色谱-串联质谱法同时测定水果中11 种农药残留 ··················································································· 王子剑，赵劲松，郭晓宇，李 倩，郑天驰，商爱媛，范 赛 （ 23 ）

藏药诃子质量标志物诃黎勒酸的标准化分析研究 ······························································································· 宋志博，陈 涛，王肖波，王岱杰，申 诚，王 硕，李洪梅，海 平，李玉林 （140）

敦煌莫高窟壁画地仗层可溶盐迁移过程模拟研究 ························ 钱 玲，吕功煊，胡红岩，陈港泉 （149）

场发射扫描电子显微镜观测弱导电金属有机框架材料的参数探究 ······························································································································· 邢宏娜，常 帅，冯 伟，李兴华 （160）

一价/二价阳离子浓度对蛋白质-核酸液液相分离的调控 ················ 刘柱梁，郑 寓，周诗航，王艳伟 （170）

碱性嫩黄O 的光电脱色工艺研究 ····························································································································· 倪赛迪，林秋涵，何碧珊，陈晓达，郭妙柃，栗鹏辉，林佳丽，陈毅挺 （178）

离子色谱法同时测定硫酸氢氯吡格雷中甲酸残留及硫酸盐含量 ·································································································································· 冯顺卿，卓文珊，王潇洋，刘洪涛 （185）

直链淀粉三(3, 5-二甲基苯基氨基甲酸酯)-聚醚砜手性膜色谱研究 ···················································································································· 普 娜，赖亚琳，高顺秋，蒋雪菲，袁黎明 （280）

蒙药十八味欧曲丸中游离汞的含量测定 ···································· 马 蕊，丁玉竹，哈 伟，师彦平 （286）

基于镍钼硫化物纳米花修饰碳纳米管的脑利钠肽电化学免疫传感器的构建 ··················································································································· 李 燕，朱长慧，代玉雪，李志英 （292）

顶空气相色谱-电子捕获检测器法测定明胶空心胶囊中2-氯乙醇残留量 ························································································································ 程 磊，郭文旭，王丹丹，陈 超 （299）

超声萃取-气相色谱法测定拟南芥种子中脂肪酸含量 ···················· 宜原原，罗 云，阮梅林，雷 敏 （339）

材料孔隙率测试方法的研究 ···················· 陈佩丽，宋 达，邓金林，范明旸，陈晓丽，付 娟，苏秋成 （347）

基于X射线光电子能谱的绝缘栅双极型晶体管失效分析 ································································································································ 章小余，赵志娟，刘 芬，徐 鹏，屈宝龙 （352）

星状风毛菊药材分析及质量标准研究 ·············································································································· 马家麟，王 硕，陈 涛，宋 霞，乔亚玲，杲秀珍，申 诚，海 平，李玉林 （357）

* 大型仪器功能开发

正负压一体式无空气X射线光电子能谱原位转移仓的开发及研制 ······························································································································· 章小余，赵志娟，袁 震，刘 芬 （ 30 ）

模拟空间原子氧辐照下X射线光电子能谱仪的原位表征功能开发 ······························································································································· 刘 建，剡 珍，郝俊英，刘维民 （ 37 ）

高低温环境下红外光谱原位表征系统的研制 ···················· 郭 艳，许传芝，王 嘉，张乐芬，牛建中 （ 43 ）

一种液体吸附原位红外表征系统 ··································· 郭 艳，许传芝，王 嘉，张乐芬，牛建中 （216）

近红外轻质油品快速检测系统的研制和应用 ······························································ 陈国钰 （221）

X-射线单晶衍射仪XtaLAB Pro 的低温系统改造 ···································· 马 宣，孙爱君，张 云 （227）

自补偿型双摆式干涉仪的设计 ················································ 石 磊，孙长库，夏恒新，李岩松 （304）

* 大型仪器科学管理

高校仪器共享平台档案信息化管理模式探索 ······························ 李艳伟，盛弘强，方三华，刘 丽 （ 49 ）

我国民营第三方检测服务现状及趋势 ···························································· 张志强，王丽红 （334）

校级分析测试中心大型仪器设备共享平台建设探讨——以西南交通大学分析测试中心为例 ·················································································································· 卫飞飞，方维臻 （429）

“四个最大”和“四个最小”的大型精密贵重仪器全生命周期管理体系的构建 ················· 薛青松 （438）

* 浙江省大型科研仪器开放共享平台—质谱专栏

牛奶中全氟烷基酸的简便萃取与定量研究 ············································ 李城华，汪 嫣，蒋可志 （ 54 ）

基于串联质量标签定量质谱法的胶质瘤外泌体蛋白组差异分析 ··························· 裴顺琪，谭 舟 （ 63 ）

基于气相色谱三重四极杆质谱法分析5 种苯系物在贻贝体内的分布、蓄积和消除规律 ················································································ 晁铎源，宋立玲，王红光，丁 顒，邵宏宏，周秀锦 （ 68 ）

Cocktail 探针药物法评价玄参对大鼠细胞色素P450 酶的影响 ····································································································· 魏艳丽，应晓倩，谈文状，吴美玲，江悦娟，丁明星，杜洪建 （ 76 ）

质谱在金属有机框架材料结构与应用表征上的研究进展 ·························· 陈银娟，丁传凡，卢星宇 （ 83 ）

质谱分析在变压器所用矿物绝缘油成分分析中的应用 ·················································· 刘佳蓉 （ 93 ）

离子色谱法测定废水中的六氟磷酸根 ······································································· 赵 薇 （101）

* 分析测试经验介绍

加速溶剂萃取-QuEChERS-气相色谱质谱联用法测定土壤中增塑剂 ······················· 唐会智，宋冬梅 （105）

原位变温X射线衍射测试技术及其影响因素 ········· 毛 晶，郭倩颖，马利利，龙丽霞，韩雅静，马晓晖 （111）

会理地区种植基地果蔬中农药残留现状与分析 ··································· 陈明华，曾 艳，欧阳卫民 （117）

综合物性测量系统振动样品磁强计测量定中心问题的探究 ······················· 马 麟，王 朔，王 维 （191）

利用Visual Basic 自动编制分析测试报告 ·································· 傅泽华，王如海，孙玉芳，唐昊冶 （197）

激光共聚焦显微镜测量表面粗糙度的探究 ············································ 廖奕鸥，冯 辉，张重远 （203）

不同参数优化对ZSM-5 分子筛的扫描电子显微镜图像影响 ································ 王馨楠，高占明 （209）

木质纤维素材料前处理的方法 ····································································· 王小曼，王 闻 （309）

无窗X射线能谱在荧光样品与金属锂成分分析中的优势与经验摸索 ·················································································· 万 鹏，蔡 蕊，李 勇，孟祥玉，周雨萌，高晓霞，徐 强，闫 肃 （313）

测量系统分析在大米镉、铅元素检测中的应用研究 ······················ 韦 冰，蒋菊媛，覃均生，张倩勉 （321）

电感耦合等离子体质谱法测定镁合金中的痕量元素 ····················································· 黄丹宇 （328）

QuEChERS-高效液相色谱/三重四极杆质谱联用法测定化妆品中防晒剂的检测方法 ···················································································· 潘秀丽，邵长春，李 赟，许晓辉，王小乔，张虹艳 （384）

熟地黄的炮制及有效成分和微量元素的检测研究 ···················································································································· 陈胜强，杨克培，康文利，周永昌，陶思曼，关伊辰，蒲秀瑛 （392）

粉末样品制备方法对扫描电子显微镜成像质量的影响 ·················································· 王馨楠 （400）

微波灰化-电感耦合等离子体发射光谱法测定婴幼儿乳粉中的钙和磷 ······································································································ 陈丽梅，张 慧，白国涛，马彩霞，姚思雨，王 婧 （407）

苯系物相对质量校正因子的测定与比较分析 ··················································· 李紫腾，李 盼 （414）

高效液相色谱法测定化妆品中类视黄醇含量 ······························ 羊洁芳，楼美娟，卢 力，姜士磊 （421）

* 综 述

基于金属有机框架材料的酶固定化策略及药物筛选研究进展 ··························································································· 常香蕾，张 瑛，Stanislas Nsanzamahoro，王铖博，王伟峰，杨军丽 （125）

行波离子迁移谱技术及应用研究进展 ························································································································· 潘慢慢，李 杭，徐一仟，杨其穆，蒋丹丹，王卫国，陈 创，李海洋 （231）

原位高分辨微区元素分布特征检测技术的应用进展 ····················· 林梵宇，尹希杰，刘建鑫，孙延鑫 （245）

便携式毒品传感器的应用与研究进展 ······································································· 杨 春 （261）

紫外光化学蒸气发生技术综述 ··························· 郭 炜，刘美彤，张卫宏，葛迎吉，康 宁，刘子杰 （272）

地下建筑内氡分布与去除技术研究进展 ··············································· 吕功煊，甄文龙，宁晓峰 （364）

* 大型仪器维护与维修

EA3000-CHNS 测试的影响因素与解决方案 ······························· 郭 毅，张滢滢，张歆宁，倪旭峰 （378）